Xue Zhong-jun
2005
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Journal
Chinese Journal of Synthetic Chemistry
Abstract
Bromoindole(3) was prepared from N,N-dimethylformamide dimethyl acetal. 4-Bromoindole-3-carboxaldehyde(4) with total yield of ~62.0% was synthesized by Vilsmeier reaction between 3, N,N-dimethylformamide and POCl_3. The structure of 4 was confirmed by 1H NMR and IR.