Zhang Zhen-xue
2011
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Journal
Journal of Shenyang University of Chemical Technology
Abstract
4-Phenylthiobenzyl chloride was prepared by the substitution of 4-fluorobenzaldehyde with thiophenol to obtain 4-(phenylthio)benzaldehyde,and then reducted with sodium borohydride and chlorination with concentrated hydrochloric acid in an overall yield of 88 %(based on thiophenol).The purity was 95.8 %.The structure and purity of target product were confirmed by HPLC,1H-NMR and MS.