Zhang Yu-mina
2010
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Journal
Chemical Reagents
Abstract
4-tert-Butyl-benzaldehyde was synthesized from 4-tert-butyl toluene via oxidation by Mn2O3 and MnO2,benzyl halide hydrolysis,the Sommelet reaction and oxidation of IBX,respectively.The influence of various factors on formation of 4-tert-butyl-benzaldehyde by oxidation in the presence of MnO2 was predominantly studied.The optimum synthetic conditions were determined,while other methods for synthesizing 4-tert-butyl-benzaldehyde were also explored,among which the IBX oxidation method could lead to a highest product yield of 86%.