Meng Fan-hao
2012
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Journal
Chemistry & Bioengineering
Abstract
5-Bromo-2-isobutoxybenzonitrile was synthesized with an overall yield of 47.7% via a three-step procedure as bromination,cyanidation and alkylation,using salicylaldehyde as starting material.The structure of the product was confirmed by 1HNMR and MS.The process was suitable for industrial preparation because of its advantages of mild reaction conditions,facile operation and relatively lower cost.