Gao Zhao-chan
2013
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Journal
Chemical Reagents
Abstract
5-Bromo-3-[( 3,4,5-trimethoxy-phenyl) thio]-1Hindole was synthesized via NBS-promoted the reaction between 5-bromo-1H-indole and 1,2-bis( 3,4,5-trimethoxyphenyl) disulfide in the solvent DMF. High yield could be obtained at room temperature without the use of metal catalyst and other additives. Starting raw could be easily available and post-treatment operation was simple. The structure of the target product was confirmed by NMR and MS.