Xian Yu-jian
2008
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Journal
Technology & Development of Chemical Industry
Abstract
The 2,6-bis(hydroxymethyl)-4-methy phenol was synthesized with p-cresol as material.Under the room temperature,2,6-bis(hydroxymethyl)-4-methy phenol was oxidized by activated manganese dioxide to synthesize 5-methyl-2-hydroxyisophtha-ladehyde.The influence factors were investigated. When the ratio of C9H12O3/ MnO2/CHCl3 was 5.0g/40.0g/250mL,reaction time was 36h,the yield was the best.