Luo Xu-qiang
2010
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Journal
Chemical Research
Abstract
4-Chlorobenzyl chloride and diethyl malonate were used as the starting materials to synthesize 6-chloro-1-indanone via condensation,alkaline hydrolysis,decarboxylation,acyl chlorination,and Friedel-Crafts acylation reaction.The target product was obtained at a total yield of 62% and with a purity of 99%.Moreover,the structure of the product was characte-rized by means of 1H-nuclur magnetic resonance spectrometry,mass spectrometry,and elemental analysis.