Kodjo Charles Guillaume, Kangah Niameke Jean-Baptiste, O. Adama
Nov 1, 2017
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Journal
International Journal of Chemical Studies
Abstract
The title compound have been synthesized and characterized by routine MS, IR and NMR spectrometry methods. Single crystal X-ray diffraction analysis showed that N,N'-bis(4-nitrophenylmethylene)hexane1,6-diamine compound crystallized in monoclinic P21/c space group with a = 6,1569(7)Å, b = 5,0751(5)Å, c = 30,631(4) Å, β = 94,509(7)° and z = 2. Crystal data were collected using Enraf-Nonius CAD4 X-ray diffractometer with monochromatic Kα radiation of Cu (λ = 1.54187Å). The structure was solved by direct methods and refined on F2 by full-matrix least-squares procedures to the final R1 of 0,152, using SHELXL programs. Crystalline network cohesion of this compound was essentially assured by C-H...O hydrogen bounds and dipole-dipole type interactions. Biological investigation carried out according DPPH and ABTS methods, revealed that this compound had antioxidant activity.