Song Hong-rui
2010
Citations
0
Influential Citations
0
Citations
Journal
Fine Chemical Intermediates
Abstract
3-Methoxy-4-acetoxy-benzoyl chloride (5) was obtained from vanillin via oxidation,esterification and chlorination.Compound 5 reacted with bromhexine to give brovanexine hydrochloride.The structure of target compound was confirmed by LC-MS,IR and 1H NMR.The synthetic route was simple and efficient to give the product in 49.7% overall yield.