Jin Zi-lin
2009
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Journal
Chemical Reagents
Abstract
2,6-Dimethyl-4-bromoaniline and 2,6-diisopropyl-4-bromoaniline were synthesized via the reaction of 2,6-dimethylaniline and 2,6-diisopropylaniline with liquid bromine.By controlling properly the reaction temperature,reaction time and feeding mode the yield of 2,6-dimethyl-4-bromoaniline and 2,6-diisopropyl-4-bromoaniline was 67% and 64%,respectively.The structures of target compounds were characterized by 1HNMR.