Chen Xue-xi
2013
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Journal
Chemistry & Bioengineering
Abstract
In this paper,using 3,3,3-trimethoxy propionitrile as raw material,3-amino-5-methoxyisoxazole was synthesized through a two-step reaction.The main influencing factors(oxygen,stirring time,light,etc.)on the synthesis were investigated by the single factor experiment.The structure of the product was characterized by 1HNMR.Under the optimum conditions,the yield and the purity of 3-amino-5-methoxyisoxazole reached 79.35%,98.91%,respectively.