A. Banaei, Soheyla Karimi, Negar Nurbageri
Oct 1, 2016
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Journal
Iranian Chemical Communication
Abstract
New 6-(hydroxymethyl)-14,16-dimethyl-13,14,16,17-tetrahydro-6H-13,17epiminodibenzo[e,l][1,4]dioxacyclotridecin-15(7H)-one(2a) was synthesized in good yield by the Petrenko-Kritchenko reaction of 2,2'-((3-hydroxypropane-1,2-diyl)bis(oxy))bisbenzaldehyde(1a) with diethyl ketone in the mixture of ethanol and acetic acid as solventin the presence of ammonium acetate. The compounds were characterized by elemental analyses, IR, H-NMR, C-NMR and mass spectrometry.