Zeng-Xia Zhao
2001
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Journal
Journal of Beijing University of Chemical Technology
Abstract
p Chlorophenylacetic acid was synthesized by the hydrolysis reaction of p chlorobenzyl cyanide in the alkaline aqueous solution with the presence of C 6H 5CH 2(CH 3) 3N +Cl - as phase transfer catalysts. The factors which affect the yield of hydrolysis reaction were studied by orthogonal experiments, and a handy method of preparation for p chlorophenylacetic acid was proposed. The compositions and structure were characterized by melting point analysis,IR,MS, etc.