C. E. Reck, C. Winter
Sep 30, 1997
Citations
0
Influential Citations
8
Citations
Journal
Organometallics
Abstract
The synthesis of 1,4-bis(chloromagnesio)-2,5-di-tert-butylbenzene was conducted by treating 1,4-bis(chloromercurio)-2,5-di-tert-butylbenzene with methylmagnesium chloride. The dimagnesiated compound was characterized by hydrolysis, halogenation, and treatment with allyl bromide. NMR spectra suggest that 1,4-bis(chloromagnesio)-2,5-di-tert-butylbenzene exists as a mixture of oligomers.