Zhang Ming
2003
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Journal
Journal of Suzhou University
Abstract
Highly pure 2,3dichlorobenzoyl cyanide was synthesized by a modified approach, in which a controlled reaction of dichlorobenzoyl chloride with cuprous cyanide was conducted directly, without using any organic solvent. FTIR,1H NMR and13C NMR presented the evidences of the structure. The results of high performance liquid chromatography (HPLC) and element analysis showed that the final product was of high purity degree.