Wang Hou-an
2010
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Journal
Journal of Anhui University of Science and Technology
Abstract
The single crystal Fe(acac)3 was successfully synthesized using acetylacetone and ferric oxide as the starting materials.The number of acetylacetonate in CCDC is 693046.It was characterized by IR,UV-Vis and X-ray single crystal diffraction.The result indicated that the crystal has an orthorhombic structure with space group Pbca and the crystallographic data of the complex are : a = 1.549 4(5)nm,b = 1.359 5(5)nm,c = 1.658 9(5) nm,α=β=γ=90°,V =3.494(2) nm3,Fe(Ⅲ) ion is coordinated with six oxygen atoms from three Hacacs,and form a slightly distorted octahedron coordination geometry.