Wang Ming-gang
2012
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Journal
Chemical Reagents
Abstract
Perfluorohexyl iodide has been used as a raw material in preparing 3-perfluorohexyl-1,2-epoxypropane(PFOP) by one-pot reaction.The total yield reached 79.6%.Starting from 3-perfluorohexyl-1,2-epoxypropane,five novel methacryloyl monomers containing aromatic rings and short perfluorocarbon side chains were obtained;and the optimal conditions of the intermediates were discussed.The monomers were confirmed by 1HNMR,13CNMR and 19FNMR.