Fengping Xiao
2013
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Journal
Chinese Journal of Spectroscopy Laboratory
Abstract
4-Trifluiormethoxy phenyl isocyanate(2)was synthesized by 4-(trifluorome-thoxy) aniline and triphosgene.Then,triflumuro(1)was synthesized by2and 2-chlorobenzamide.The overall yield was 84.7%.Analysis of1was determined by HPLC and the purity of1is up to 99%.The structure of the product was identified by IR,1HNMR and elemental analysis.