Baolei Wang, Xing-hai Liu, Zhengming Li
Sep 4, 2009
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Phosphorus, Sulfur, and Silicon and the Related Elements
Abstract
Several novel trichloromethyl-containing O,O-dimethyl phosphoramidothioate derivatives have been synthesized by the reaction of O,O-dimethyl phosphoramidothioate with chloral imines. The latter were prepared in good yields by refluxing the dichloroethane solution of chloral and substituted anilines using 3 Å molecular sieves as dehydrating agent. Structures of title compounds were confirmed by IR, 1H NMR, 31P NMR, and FT-MS studies.