T. Zhu
2010
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Journal
Journal of Guizhou University
Abstract
Starting with pentaerythritol,2,2-Bis(bromomethyl)-1,3-propanediol was synthesized with the improved method.An aldol condensation between 2,2-Bis(bromomethyl)-1,3-propanediol and PQAB was carried out.The target product 4-(2,6-dioxaspiro-4,4-dibromomethylcyclohexyl)-N,N-dimethylaniline was obtained.The new compound was well-characterized including MS,IR,1H NMR spectroscopy,and X-ray single crystal diffraction.