M. J. Fernández, R. Huertas, E. Gálvez
Sep 15, 1995
Citations
0
Influential Citations
6
Citations
Journal
Journal of Molecular Structure
Abstract
Abstract A series of amides derived from 3,7-dimethyl-3,7-diazabicyclo[3.3.1]nonan-9-amine ( I ) have been synthesized and examined by IR, 1 H and 13 C NMR spectroscopy, and the crystal structure of 9-(3-indolycarboxamido)-3,7-dimethyl-3,7-diazabicyclo[3.3.1]nonane hydrochloride ( IV ·HCl) has been determined by X-ray diffraction. The 1 H and 13 CNMR data of the parent amine ( I ) are also included. These compounds adopt an almost perfect chair-chair conformation with the NCH 3 groups in the equatorial position