Salima M. Abosaadiya, B. Yamin, Aishah Hasbullah
Nov 17, 2016
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Abstract
1,1’-Bis(2-bromobenzoylthioureido)ethane was synthesized from the reaction of 2-bromobenzoylisothiocyanate and ethylenediamine in acetonitrile. The compound was characterized by FT-IR, 1H, and 13C NMR spectroscopy techniques. Furthermor compound was found to crystallized in monoclinic system with space group of P2(1)/c. In each thiourea moiety the thiono group is trans to the benzoyl across their C-N bonds. The crystal structures are stabilized by N–H···S intermolecular hydrogen bonds to form infinite two dimensional network.