Wang Zongde
2012
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Journal
Journal of Jiangxi Normal University
Abstract
A new camphene acid amide was synthesized from camphene via the Vilsmeier-Haack reaction,oxidation,acylation and amidation.The structure of the product was characterized by IR,elemental analysis and single crystal X-ray diffraction.The product belongs to triclinic system,P21/c space group,with a = 1.220 0(9) nm,b = 0.803 6(6) nm,c = 1.065 4(8) nm,α = 90.000°,β = 96.981(9)°,γ = 90.000°,V=1.036 8(13) nm3,Dc=1.161 g.cm 3,Z = 1,μ = 0.073 mm 1,F(000) = 400,S=1.080,R1=0.082 9,wR2=0.182 9.The 3D hydrogen bonding network structure is constructed via the intermolecular N—H…O hydrogen bond interactions.