Lin Chun-ling
2012
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Journal
Journal of Xi'an Shiyou University
Abstract
The monosodium salt of 2,4,6-trimercapto-s-triazine Na(H2O)3C3H2N3S3 was synthesized by the reaction of C3N3Cl3 with Na2S and NaOH in the solution of pH=5~8,and it is characterized by IR spectrum and element analysis.Its structure is determined by X-ray diffraction analysis.The salt crystallizes in the monoclinic space group P2(1)/c with a=10.479(4),b=12.761(5),c=7.822(3),β=109.623(6)°,V=992.8(7).3,Z=4,Dc=1.695 g·cm-3,R1=0.044 4,wR2=0.136 0(I2),GOF=1.128.