Z. Ping
2007
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Journal
Journal of Wenzhou University
Abstract
N-(2,6-dichloro-4-thrifloromethylphenyl)acetamide was synthesized from the reaction of 2,6-dichloro-4 –trifloromethylaniline with POCl3 in acetate.The structure of the title compound was determined by 1H NMR,13C NMR,19F NMR,IR and X-ray diffraction analysis.Crystal data: monoclinic,space group C 2/c,a =19.739(2)■,b =12.0183(14)■,c =9.6533(12)■,α=90°,β=106.364(2),γ=90°;Z=8,F(000)=1088,R1=0.06.