Z. Qian
2009
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Journal
Chinese Journal of Synthetic Chemistry
Abstract
A novel carbazole derivative,(E)-(9-ethylcarbazol-3-yl)-N-(3,5-dimethyl-1,2,4-triazol-4-yl)-methanimine(1),was synthesized by reaction of 3-aldehyde-9-ethylcarbazole and 4-amido-3,5-dimethyl-1,2,4-triazole.The structure was characterized by 1H NMR,IR and X-ray single-crystal diffraction.1 belongs to monoclinic system,space group P2(1)/n with a=8.829(8) ,b=9.863(10) ,c=19.530(15) ,β=101.65(5)°,V=1 666(3) 3,Dc=1.266 g·cm-3,Z=4,F(000)=672,μ=0.079 mm-1.The final R1 indices was 0.075 6.