X. Zhang, Y. Dong, W. Chen
Feb 25, 2015
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Phosphorus, Sulfur, and Silicon and the Related Elements
Abstract
GRAPHICAL ABSTRACT Abstract Triethylammonium 2,4,14,16-tetrachlorodibenzo[g,j][1,3,6,12]tetraoxacyclotetradecane-2-phosphorodithioate was synthesized from bis(3,5-dichloro-2-hydroxyethoxyphenyl)methane by a two-step one-pot sequence. Its structure was confirmed by 1H, 13C, and 31P NMR spectra, and elemental analysis. The X-ray diffraction analysis indicated that the molecules of the compound form an inclusion complex with chloroform molecules outside the phosphorus-containing macrocycle in the ratio of 1:2.