Yq Yin, Zhijuan Yu, Yl Zhang
Dec 15, 2012
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Abstract
The title compound 1-[2-(3-ethyl-2,2-dimethylcyclobutyl)acetyl]-3-phenylthiourea has been synthesized and its crystal structure was studied. The crystal belongs to triclinic system, space group P -1, a = 10.200(2) Ǻ, b = 12.395(3) A, c = 15.679(3) A, α = 92.99(2) o , β = 106.00(3) o , γ = 111.95(3) o , V = 1740.4(6) A 3 , Z = 2, μ = 0.187 mm −1 , D c = 1.162 g/cm 3 , F (000) = 656, R = 0.0784, wR 2 = 0.1505, formula unit C 17 H 24 N 2 OS. The title compound has a fragment of 2,2-dimethylcyclobutane and its conformation represents semi-chair . The intermolecular and intramolecular hydrogen bonds are revealed. KEY WORDS : Synthesis, Single crystal X-ray diffraction, Crystal structure, 2,2-Dimethylcyclobutane Bull. Chem. Soc. Ethiop. 2013 , 27(1), 125-129. DOI: http://dx.doi.org/10.4314/bcse.v27i1.13