Li-xia Zhao, Ying Fu, F. Ye
Jul 1, 2011
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Abstract
Abstract The title compound, (R)-(-)-N-dichloroacetyl-3-ethyl-1-oxa-4-aza-spiro-4.5-decane 3 was synthesized by a sequential procedure involving condensation of (R)-2-amino-butanol with cyclohexanone and acylation of the resultant intermediate spiro compound with dichloroacetyl chloride. The X-ray structure determination confirmed the structure and the product was further characterized by IR, 1H-NMR, and 13C-NMR spectroscopy, mass spectrometry, and elemental analysis.