Hui Zheng, Yunkui Liu, Chao Shen
Jun 19, 2009
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Journal
Journal of Chemical Crystallography
Abstract
A new compound having potential bioactivities 3,5-dichloro-6-morpholinopyridin-2-ol (1) was synthesized and characterized by single crystal X-diffraction. The crystal is monoclinic, space group P21/c with a = 10.3609 (6), b = 10.5711 (7), c = 10.3190 (5) Å, β = 108.9433 (15)°, V = 1068.99 (11) Å3, Z = 4, C9H10Cl2N2O2, Dc = 1.548 g/cm3, μ (MoKα) = 0.71075 Å, S = 1.01, F (000) = 512.00, R = 0.0397 and wR = 0.1364. In the unit cell, there are two independent molecules linked by intermolecular O–H···O (2.693(2) Å) hydrogen bonds forming onedimensional expanded structure.Graphical AbstractAs part of our ongoing research work on pyridine derivatives, the title compound crystal structure is important to study the relationship between the structure and its biological activities, thus it is urgent to publish in time.