S. Sharma, M. Sharma, R. Rathee
2006
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0
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Journal
Journal of the Indian Chemical Society
Abstract
A convenient synthesis of geranyl N-dimethylallylanthranilate 1, utilizing DMAP mediated esterification of isatoic anhydride 2 with geraniol 3 and subsequent N-alkylation of the resulting ester 4 using tetrabutylammonium iodide with 3,3-dimethylallyl bromide 5 has been achieved in 88.2% yield. The identity with the naturally occurring compound was established on the basis of 1 H NMR and 13 C NMR data.