Song Hao
2011
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Journal
Chinese Journal of Synthetic Chemistry
Abstract
A key anti-cancer drug intermediate,t-butyl{1-[(p-phenylacetyl)phenyl]cyclobutyl}carbamate,was synthesized in yield of 33% by the Weinreb ketone synthesis method of t-butyl[1-(p-bromophenyl)cyclobutyl]carbamate with N-methyl-N-methoxy-2-phenylacetamide in the presence of n-BuLi.The structure was confirmed by 1H NMR.