Fan Guorong
2012
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Journal
Applied Chemical Industry
Abstract
Hydronopyl benzyl ether,a novel compound,was synthesized from the reaction of hydronopol and benzyl chloride in sodium hydroxide solution with the existence of tetrabutylammonium bromide(TBAB),benzene as solvent.The reaction conditions were optimized by single factor experiment.The optimum synthetic conditions were hydronopol∶benzyl chloride∶sodium hydroxide=1∶2∶4(molar ratio),the content of sodium hydroxide in solution 50%(mass fraction),reaction time 7 h.Structure of the product was identified by IR,1H NMR,13C NMR.