Tang Li-jua
2015
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Journal
Journal of Huaihai Institute of Technology
Abstract
The novel compound ethyl-2-(benzenepeptide-5-yl)-4-methyl-1,3-thiazole-5-carboxylate has been designed and synthesized by the cyclization of thioamide with 2-chloroacetoacetate,and the yield of the process is above 60%.5-Thioamide benzene was prepared by the reaction of 5-cyanophthalide with 17% ammonium sulfide with the yield of 89.6%.The structures of the products were established by IR,~1H NMR and MS spectra.