Xue Feng
2005
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Journal
Chinese Journal of Pharmaceuticals
Abstract
Methyl 1H-1,2,4-triazole-3-carboxylate was synthesized from 1H-1,2,4-triazole by hydroxymethylationwith formaldehyde in presence of Ba(OH)2·8H2O to give 3-hydroxymethyl-1H-1,2,4-triazole followed by oxidation andesterification with an overall yield of 32% and purity of 98%.