Shi Qunfeng, Z. Weiwei, Zhou Heng
2012
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Journal
Chinese Journal of Pharmaceuticals
Abstract
Methyl 4-fluoro-3-methylpyridine-2-carboxylate(1) was synthesized from methyl 3-methylpyridine-2-carboxylate(2) by oxidation,nitration and reduction to give methyl 4-amino-3-methylpyridine-2-carboxylate(5),followed by modified Balz-Schiemann reaction with an overall yield of about 18%(based on compound 2).