E. A. Monin, I. A. Bykova, E. A. Chernyshev
May 1, 1993
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Journal
Russian Chemical Bulletin
Abstract
Abstract(Methylchlorosilyl)methyldichlorophosphines have been synthesized by the reaction of [dimethy(diethylamino)silyl]- or [methyl-bis(diethylamino)silyl]methylmagnesium chlorides with PCl3 in ether at −40÷−20 °C and subsequent treatment of the reaction mixture with dry HCl. The structures of the compounds thus obtained have been studied by31P,1H, and13C NMR spectroscopy.