Liu, Tian-bao, Peng
2008
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Journal
Chinese Journal of Structural Chemistry
Abstract
The title compound 2,4-chloromethyl-3-anilino-2-(4-methyl-benzoylimido)thiazole,was prepared by the reaction of 1-p-methylbenzoyl-3-phenylaminothiourea 1 with 1,3-dichloroacetone.The crystal is of monoclinic,space group P21/c,with a = 8.1712(15),b = 10.998(2),c = 19.134(4),β = 94.610(5)o,C18H16ClN3OS,Mr = 357.85,Z = 4,V = 1714.0(6) 3,Dc = 1.387 g/cm3,μ(MoKα) = 0.354 mm-1,F(000) = 744,the final R = 0.0518 and wR = 0.1167 for 3189 observed reflections(I 2σ(I)).Its formation mechanism was proposed.