Jianling Zhao, Xixin Wang, Chaoya Liu
Apr 9, 2008
Citations
0
Influential Citations
7
Citations
Journal
Powder Technology
Abstract
Abstract Nearly monodisperse antimony pentoxide with a mean diameter of 2 nm and polydispersity of 0.047 was prepared through a simple method based on reflux oxidization system. By adjusting the synthetic parameters (kinds of stabilizing agents, size and purity of original Sb 2 O 3 etc.), the controllable synthesis of ultrafine Sb 2 O 5 can be easily achieved. Detailed investigations about the effects of experimental parameters on the colloid stability and size distribution of the final products were carried out. The particles were characterized using various experimental techniques such as transmission electron microscopy (TEM), X-ray diffraction (XRD) and particle size distributions.