Ma Xiao-qi
2015
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Journal
Chinese Journal of Synthetic Chemistry
Abstract
A natural product,N,N'-diferuloyl-putrescine( 1),was prepared by condensation reaction of ferulic acid with 1,4-diaminobutane. First total synthesis of JBIR-94 with total yield of 77. 1% was accomplished by reduction of 1 using Pd / C as the catalyst. The structures were confirmed by1 H NMR,13 C NMR and IR.