P. Ferraboschi, P. Grisenti, Enzo Santanitllo
Mar 1, 1994
Citations
0
Influential Citations
3
Citations
Journal
Journal of Labelled Compounds and Radiopharmaceuticals
Abstract
The acid catalyzed reaction of glycerol-d5 with bromoacetaldehyde dimethyl acetal affords the corresponding 2-bromomethyl-4-hydroxymethyl-1,3-dioxolane, which was treated with lithium iodide in 2-butanone to afford the pentadeuterated domiodol 1 in high isotopic purity.