M. Iwanami, T. Numata, M. Murakami
1968
Citations
2
Influential Citations
23
Citations
Journal
Bulletin of the Chemical Society of Japan
Abstract
By the hydrolysis of pyridoxal-5-phosphate Schiff bases, pyridoxal-5-phosphate was prepared in a crystalline form without any further purification. Pyridoxal-5-phosphate Schiff bases were prepared in good yields by the phosphorylation of pyridoxal Scruff bases and were easily purified by alkali-acid reprecipitation. The pyridoxal-5-phosphate thus obtained was demonstrated to be identical with an authentic sample by a study of its UV, IR, and NMR spectra.