Rabeya Khatun, A. Islam, M. Hai
Sep 2, 2012
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Abstract
Syntheses of Schiff’s base 1 1-[(2, 4-difluorophenyl)-2-(1H-1, 2, 4-triazol-1-yl)] ethanone thiosemicarbazone ( 1A ) prepared by condensation of 1-(2,4- difluorophenyl)-2-[1(H)-1,2,4-triazol-1-yl] ethanone with thiosemicarbazide, followed by cyclization 2 to 2-(2,4-difluorophenyl)-2-[(1H)-1,2,4-triazol-1- ylmethyl)]-3-acetyl-5-acetylamino- thiadiazoline ( 2A ), using acetic anhydride, and finally hydrolysis 3 of ( 2A ) to form 2-(2,4-difluorophenyl)-2-[(1H)-1,2,4-triazol-1- ylmethyl)]-3-acetyl-5-amino-thiadiazoline ( 3A ), using hydrazine hydrate, all compounds having anti-fungal activities, are reported. DOI: http://dx.doi.org/10.3329/jbcs.v25i1.11765 Journal of Bangladesh Chemical Society, Vol. 25(1), 7-14, 2012