S. Saeed, N. Rashid, M. Bhatti
Nov 30, 2010
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Journal
Turkish Journal of Chemistry
Abstract
N-{[(4-bromophenyl)amino]carbonothioyl}benzamide was synthesized and characterized by IR, Hand C-NMR, mass spectrometry, and elemental analysis. The crystal structure was determined from single crystal X-ray diffraction data. It crystallizes in monoclinic space group P21 /n with unit cell dimensions a = 13.822(3) A, b = 5.927(2) A, c = 16.642(3) A, and β = 103.963(3)◦ . There is a strong intramolecular hydrogen bond of the type N HΛO, with an HΛO distance of 2.6129 (11) A. The mass fragmentation pattern is also discussed.