S. Jia
2010
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Journal
Chinese Journal of Spectroscopy Laboratory
Abstract
The key intermediate 2,3,4,5-tetramethoxytoluene(TeMT) was synthesized from 3,4,5-trimethoxy-benzaldehyde as the raw material by Wollf-Kishner-Huangminglong reaction,selectively bromination.The title compound was prepared by the selective oxidation of CAN and TeMT.The overall yield of the route is 81.0%.The route is noted for easily afford of the raw material,high yield,easy procedure,and environment friendly.