Z. Ming-gen
2008
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Journal
Journal of Shanxi University
Abstract
A new compound,4-chloro-2,2-dicyano-N-chloroacetyl butanamide-3-ketone,was synthesized by the reaction of potassium monocarbamoyl-dicyano-methide with chloroacetyl chloride through surface contact method of solid-liquid phase under room temperature.The reaction yield was 11.2% and the melting point of the product was 147.8 ℃~148.1 ℃ The molecular structure was characterized by IR and 1HNMR.