Lin Xi
2011
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0
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Journal
Chinese Journal of Spectroscopy Laboratory
Abstract
1-chloromethyl-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline hydrochloride was synthsized from 3,4-dimethoxy phenethylamine via acylation,Bischler-Napieralski reaction and reduction,then salt formation with muriatic acid,while overall yield was 41.1%,which has not been reported in literatures.The structure of the intermediate and target compounds were characterized by IR and 1H NMR.