C. Kazak, V. Yilmaz, E. Ağar
Jun 1, 2006
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Journal
Crystal Research and Technology
Abstract
A new 1,2,4‐triazole derivative, 3‐phenyl‐5‐p‐tolyl‐4‐(3,4,5‐trimetoxy benzilideneamino)‐4H‐1,2,4‐triazole, C25H24N4O3 (1), has been prepared by the reaction of 4‐amino3‐phenyl‐5‐p‐tolyl‐4H‐1,2,4‐triazole and 3,4,5‐trimetoxybenzaldehyde and structurally characterized by single crystal X‐ray diffraction. Compound (1) crystallizes in the monoclinic space group P21/c with a = 12.4336(11), b = 12.5860(11), c = 14.3944(14)Å, β = 94.417(7)°, Z = 4, V = 1.267 Å3. In the solid state, the molecules of (I) are discrete and not planar, comprising a twisted four‐ring system. The molecules are held together with van der Waal's interactions. (© 2006 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim)