Ashutosh Kumar Singh, Khem Raj Kandel
Dec 19, 2013
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Journal
Journal of Nepal Chemical Society
Abstract
The basic nucleus 4-(amino)-5-phenyl-l-4H-1,2,4-triazole-3-thiol has been synthesized by cyclisation of potassium dithiocarbazinate with hydrazine hydrate using water as solvent under reflux condition for 3-4 h. The compound which has been synthesized successfully was subjected to condensation with benzaldehyde to synthesize 4-(benzylideneamino)-5-phenyl -4H-1,2,4 – triazole-3-thiol (Schiff base). The compounds were confirmed by physical parameters (melting point), chromatographic methods (TLC) and spectroscopic methods (IR and NMR). DOI: http://dx.doi.org/10.3126/jncs.v30i0.9391 Journal of Nepal Chemical Society Vol. 30, 2012 Page: 174-177 Uploaded date : 12/20/2013