Wang Xiao-shan
2011
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Journal
Anhui Chemical Industry
Abstract
Objective:Synthesis of 3-(4-hydroxy-3-methoxy-phenyl)-1-piperazin-1-yl-propenone hydrochloride.Methods:The synthesis involved ferulic acid acetylation protection,then reacted with piperazine to obtain monosubstituted piperazine derivatives,then deacetylase to obtain target product.Results and conclusions:The chemical structure of 3-(4-hydroxy-3-methoxy-phenyl)-1-piperazin-1-yl-propenone hydrochloride was confirmed by IR,1HNMR and MS.The yield was over 56.9%.